Alpha spectrometry is used for qualitative and quantitative analysis of actinides in biological and environmental samples. This technique requires a thin, homogenous and carrier-free deposit. Numerous methods for source preparation are electrolytic deposition, spontaneous deposition, micro-precipitation, direct evaporation, vacuum sublimation, etc. The most widely used method for preparation of actinides for alpha spectrometry is electro-deposition of actinides onto a stainless steel planchette. This procedure is time consuming, requires elaborate equipment and is expensive. Micro-precipitation method on the other hand is comparatively faster and more reliable. Thus, the present study was taken-up to optimize various parameters for rapid alpha source preparation of actinides by micro-precipitation method.