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Author(s) |
Singh, K.; Mohan, R.; Kumar, N.; Bhattacharya, S.; Rayaprol, S.; Gaur, N. K.; Singh, R. K. |
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A systematic study on the effect of silver (Ag) doping in magnesium diboride (MgB2) superconductor has been undertaken. A series of polycrystalline samples with composition Mg1-xAgxB2 (0
£
x £
0.20) were synthesized by using the "in situ" solid state reaction method. All the samples were sintered at 850
°C for 2 h under the high purity argon flow. The room temperature X-ray diffraction (XRD), low temperature resistivity
(p-T) measurements and field emission scanning electron microscopy (FE-SEM) were performed to explore the phase purity, superconducting transition temperature, and microstructural properties, respectively. The XRD patterns show that Ag doping leads to the formation of Mg-Ag phase. The relative intensity of Mg-Ag phase increases with increasing Ag content. The
p-T measurement shows that superconducting transition temperature
(Tc) decreases slightly with Ag doping. All the samples have
Tc between 38.5K (x = 0.00) and 37K
(x = 0.20). The FE-SEM images have revealed hexagonal shaped grains with an average grain size between 0.20 and 0.50µm. |
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