BARC/PUB/10//0800

 
 

Superconducting and microstructural properties of Mg1-xAgxB2

 
     
 
Author(s)

Singh, K.; Mohan, R.; Kumar, N.; Bhattacharya, S.; Rayaprol, S.; Gaur, N. K.; Singh, R. K.

ABSTRACT

A systematic study on the effect of silver (Ag) doping in magnesium diboride (MgB2) superconductor has been undertaken. A series of polycrystalline samples with composition Mg1-xAgxB2 (0 £ x £ 0.20) were synthesized by using the "in situ" solid state reaction method. All the samples were sintered at 850 °C for 2 h under the high purity argon flow. The room temperature X-ray diffraction (XRD), low temperature resistivity (p-T) measurements and field emission scanning electron microscopy (FE-SEM) were performed to explore the phase purity, superconducting transition temperature, and microstructural properties, respectively. The XRD patterns show that Ag doping leads to the formation of Mg-Ag phase. The relative intensity of Mg-Ag phase increases with increasing Ag content. The p-T measurement shows that superconducting transition temperature (Tc) decreases slightly with Ag doping. All the samples have Tc between 38.5K   (x = 0.00) and 37K (x = 0.20). The FE-SEM images have revealed hexagonal shaped grains with an average grain size between 0.20 and 0.50µm.

 
 
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