BARC/PUB/2012/0191

 
 

Nanohardness of Sintered and Shock Deformed Alumina

 
     
 
Author(s)

Chakraborty, R.; Dey, A.; Mukhopadhyay, A. K.; Joshi, K. D.; Rav, A.; Mandal, A. K.; Bysakh, S.; Biswas, S. K.; Gupta, S. C.
(APD)

Source

Metallurgical and Materials Transactions-A, 2012. Vol. 43: pp. 459-470

ABSTRACT

To understand how high–strain rate, flyer-plate impact affects the nanohardness of a coarse (~10 μm) grain, high-density (~3.978 gm cc–1) alumina, load controlled nanoindentation experiments were conducted with a Berkovich indenter on as-sintered disks and shock-recovered alumina fragments obtained from an earlier flyer-plate shock impact study. The nanohardness of the shock-recovered alumina was much lower than that of the as-sintered alumina. The indentation size effect was severe in the shock-recovered alumina but only mild in the  as-sintered alumina. Extensive additional characterization by field emission scanning electron microscopy, transmission electron microscopy, and analysis of the experimental load depth data were used to provide a new explanation for the presence of strong indentation size effect in the shock recovered alumina. Finally, a qualitative model was proposed to provide a rationale for the whole scenario of nanoindentation responses in the as-sintered and shock-recovered alumina ceramics.

 
 
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