BARC/PUB/2023/0948

 
 

Application of conventional spray dryer to prepare nanosilica-alginate based rhodamine loaded microstructures and nanobeads

 
     
 
Author(s)

Mishra, A.; Melo, J. S.; Bhainsa, K. C.
(NA&BTD;BSG)

Source

Journal of Materials Research, 2023. Vol. 38: pp. 3362-3371

ABSTRACT

The applicability of conventional spray dryer was studied to prepare micro as well as nano carriers. Using spray drying technique rhodamine B (RhB) loaded nanosilica-sodium alginate microstructures (RhBmicrostructures) was prepared. For the preparation of nanobeads, nozzle (atomizer) of spray dryer was used to spray the feed comprising RhB-nanosilica-sodium alginate in the calcium chloride solution and RhB loaded nanosilica-calcium alginate nanobeads (RhB-nanobeads) were obtained. Prepared carriers (RhB-microstructures and RhB-nanobeads) were characterized using SEM, FTIR, DLS and Zeta potential techniques. The flowability of prepared carriers were studied using compressibility index (C.I.) and Hausner ratio (H.R.). RhB-microstructures showed a higher loading efficiency 98.6% in comparison to 46.7% of RhB-nanobeads. In vitro release study demonstrated slow and pH-responsive release of RhB from nanobeads. Present study shows the applicability of conventional spray drying and use of spraying nozzle of conventional spray dryer to prepare microstructures and nanobeads, respectively.

 
 
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