BARC/PUB/2017/1037

 
 

Amide-mediated enhancement of sorption efficiency of trivalent f-elements on functionalized carbon nanotube: Evidence of physisorption

 
     
 
Author(s)

Gupta, N. K.; Sengupta, A.; Rane, V. G.; Kadam, R. M.
(RCD)

Source

Separation Science and Technology, 2017. Vol. 52 (13): pp. 2049-2061

ABSTRACT

Amide-functionalized carbon nanotubes (CNTs) enhanced the sorption efficiency of trivalent f-elements. Different isotherm models were employed to understand the mechanism. Sorption proceeded via physisorption, and confirmed IR spectroscopy. The Electron Paramagnetic Resonance (EPR) spectra of the Gd3+ sorbed on CNT also showed no perturbation on the local environment of Gd3+ on sorption, again revealing the physisorption. Analysis of the sorption kinetics through Lagergren’s first-order kinetics, intraparticle diffusion model, and pseudo-secondorder kinetics revealed that the sorption kinetics followed pseudo-second-order kinetics. Radiolytic stability of CNT-DHA was found to be satisfactory. Ethylene diamine tetra acetic acid (EDTA) was found to strip almost quantitatively.

 
 
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